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Linear electron beam radiation has been used to induce irradiation grafting of glycidyl methacrylate (GMA), glycidyl methacrylate/β-cyclodextrin (GMA/β-CD), and glycidyl methacrylate/monochlorotriazinyl-β-cyclodextrin (GMA/MCT-β-CD) onto cotton fabrics. The effect of radiation dose, GMA concentration and CDs concentration on graft yield, epoxide content and the bonded amount of CDs was investigated. Results obtained reveal that the amount of CDs bonded within the fabric; the add-on and the epoxide content are directly related to the CDs concentration, GMA concentration and the irradiation dose. Graft yield and epoxide content increase with the increase of radiation dose to a certain extent, and they decrease due to degradation of GMA at higher irradiation doses. Results also reveal that although the bonded amount of CDs is nearly proportional to the concentration of CDs in the treatment solution, the accessibility ratio of CDs decreases with increasing CDs concentration. Treatment of fabrics grafted with GMA (Cell-g-GMA) and GMA/CDs mixtures (Cell-g-GMA/CDs) in a sequel step with the corresponding CDs increases the amounts of CDs fixed onto the fabrics, while epoxide content decreases. The treatment of the cotton fabrics with GMA and CDs was established on the basis of spectral data studies.

Incorporation of chitosan in the molecular structure of a cotton surface was effected by two approaches. The first approach involved oxidation of cotton fabric with sodium periodate (NaIO₄) and treatment of the fabric with chitosan in the subsequent step. The second approach formed the basis for devising a single-step process in which the fabric was treated in an aqueous solution containing both oxidants and chitosan. Appropriate conditions were established for a two-step process. The results of one step process were used to devise a novel one-step process in which cotton fabric containing chitosan could be achieved. This fabric exhibited significantly improved performances when compared with the untreated and processed fabric. It is assumed that NaIO₄ oxidants and chitosan enhance the interaction of chitosan with cotton by modifying the molecular structure of both.

This study aims to explore the incorporation of starch nanoparticles (SNPs) in cross-linking formulation of cotton fabrics to see their impact on fabric performance like tensile strength, dry wrinkle recovery angles, elongation at break, degree of whiteness and increase in weight as well as durability.

SNPs of size around 80-100 nm were successfully prepared from native maize starch by Nano precipitation technique and confirmed instrumentally by scanning electron microscope (SEM), transmittance electron microscope (TEM), Fourier transformer infrared (FTIR) spectroscopy and particle size analyzer. The latter were incorporated in cross-linking formulation of cotton fabrics encompassing different concentrations of citric acid and sodium hypophosphite at different curing time and temperature in 100 ml distilled water to a wet pickup of ca. 85 per cent. The fabric samples were dried for 3 min at 85°C and cured at specified temperatures for a specified time intervals in thermo fixing oven according to pad-dry-cure method.

FTIR spectra and SEM micrograph signified the chemical structure and surface morphology of cotton fabric before and after finishing in absence and presence of SNPs. Cotton fabric samples finished in presence of SNPs showed a higher tensile strength, elongation at break, comparable dry wrinkle recovery angles and degree of whiteness than that finished in their absence. On the other hand, the enhancement in the aforementioned performance reflects the positive impact of incorporation of SNPs in textile finishing especially with strength properties; which are one of the important requirements for industrial fabrics that can be used widely in heavy-duty applications.

SNPs with its booming effect with respect to biodegradability, reactivity and higher surface area can be used as a novel reinforcement permanent finish for cotton fabrics instead of more hazardous materials likes poly acrylate and monomeric compounds.

As SNPs biopolymers is one of the important reinforcement agents, so it was expected that it would minimize the great loss in strength properties during easy-care cotton finishing and improve the fabric performance.

The novelty addressed here is undertaken with a view to remediate some of the serious defects of easy-care cotton fabrics using poly carboxylic acids; especially with the great loss in strength properties by virtue of using SNPs as a permanent finish. Besides, to the authors’ knowledge, there is no published work so far concerning the use of SNPs as an innovative base for production of easy-care finished cotton textiles with high performance.

The green synthesis strategy was established for textile finishing, aiming at development of antimicrobial-printed cotton and silk fabrics. The synthesis referred to the treatment of these fabrics with chitosan of low, medium and high molecular weights using different concentrations of each. This was followed by screen printing using a natural dye extracted from prickly pears. Thus, the obtained fabrics were monitored for nitrogen, color strength and antimicrobial activity. The results signify that the chitosan concentration and its molecular weight determine the magnitudes of both antimicrobial activity and color strength. Utilization of chitosan of medium or high molecular weight at a concentration of 2% in the treating solution inhibits completely the growth of s. aureus and E. coli, which represent two types of bacteria, namely gram +ve and gram −ve. Meanwhile, the color strength assumes the highest values. The antimicrobial activities of the treated fabrics with respect to other strains of bacteria and their color strength were reported. Also reported was the mode of interactions of chitosan with cotton and silk fabrics as well as a comparison between the results obtained from these two substrates.

An alternative approach is used to cure glyoxal/β-cyclodextrin treated cotton fabric to impart a crease resistance finish. Low microwave power (200 w) for 2 min of curing time is sufficient to impart a high crease recovery angle to the fabric. Comparisons have been made for conventional/and microwave cured cotton fabric with glyoxal in the absence and presence of β-cyclodextrin. The crosslinking efficiency in conventional and microwave cured samples is evaluated on the basis of the crease recovery angle, tensile strength and elongation. The ability of β -cyclodextrin to include hydrophobic molecules, such as fragrances and antimicrobial agents (Tinosan^®) can be explored to produce new cotton fabric with unique performances. The physicochemical properties and performance of the untreated and treated fabrics are evaluated with crease recovery angles that reach about 260° and tensile strength of 42 kg, in which perfumed and antimicrobial finishings are evaluated. The modified cotton fabric is characterized with a scanning electron microscope (SEM) and Fourier transform infrared spectrophotometer (FTIR), and β-cyclodextrin inclusion with Tinosan^® improves with a 1H nuclear magnetic resonance (NMR) spectrum.

The purpose of this study is to successfully apply ultrasonic waves for the quick extraction of flax seed gum from flaxseed hull or whole seed and compare it to the standard technique of extraction.

The effect of the heating source, extracted time, temperature and pH of extracted solution on the extraction was studied. The obtained gum is subsequently used for silk screen printing on cotton, linen and viscous fabrics. Rheological properties and viscosity of the printing paste were scrutinized in the current study to get a better insight into this important polysaccharide. The output of this effort aimed to specify the parameters of the processes for printing textiles to serve in women’s fashion clothes by applying innovated handmade combinations of Islamic art motives using a quick and affordable method. Seven designs are executed, and inspiring from them, seven fashion designs of ladies’ clothes were designed virtually by Clo 3D software.

The result recorded that the new gum has excellent printing properties. In addition, they have better rheological properties, viscosity, chromatic strength and fastness qualities, all of which could help them in commercial production.

Flaxseed and three different fabric types (Cotton, Linen and Viscous) were used.

Synthesis of a new biodegradable thickener from a natural resource, namely, flaxseed, by applying new technology to save time, water and energy.

Synthesis of eco-friendly biodegradable thickener and used in textile printing alternative to the synthetic thickener.

Significant enhancement in the performance of durable press cotton fabric could be achieved through the utilization of non- formaldehyde crosslinking agents along with ionic crosslinking. Ionic crosslinking was first effected by subjecting cotton fabric succesively to partial carboxymethylation using monochloroacetic acid and sodium hydroxide, then by cationization using 3-chloro-2-hydroxypropyl trimethyl ammonium chloride known commercially as Quat-188. While the partial carboxymethylation reaction introduces the negatively charged group in the cellulose chains of cotton, the cationization reaction introduces the positively charged groups, thereby causing ionic crosslinking. The ionically crosslinked cotton was then crosslinked using either glyoxal, epichlorohydrin, or gluteral-dehyde. Most of the results obtained indicated that a balance between wet and dry wrinkle recovery angles that acquired a value as high as 300° could be obtained without loss in tensile strength and elongation at break. The results also revealed that the degree of ionic crosslinking relies on the nitrogen and carboxyl contents of the finished fabric as well as on the nature of the non-formaldehyde finishing agent used. Indeed the results of this work present a new approach to the durable press finishing of cotton, and mill trials should be conducted.

Cotton-based fabrics, namely loomstate cotton fabric, grey mercerized cotton fabric, loomstate cotton/polyester (50/50 and 35/65) blended fabric were bio-desized by α amylase enzymes and bio-scoured by alkaline pectinase enzymes. The obtained bio-scoured substrates were subject to bleaching with peracetic acid and proceeded for bio-polishing under a variety of conditions. Results show that the extent of bio-polishing depends on the conditions of the treatment. The loss in fabric weight exhibits values which are comparable at 50° and 60°C and substantially higher than those obtained at 40°C. Temperatures of bio-polishing, specifically 40° and 50°, decrease the whiteness index; higher temperature, i.e. 60 °C, does not cause further decrease in the whiteness index whereas the tensile strength decreases. The temperature has a positive effect on surface roughness particularly when bio-polishing is performed at 50°and 60 °C. It was also found that cellulase is more active in mercerized cotton than in either 100 % cotton or cotton/polyester blend. The scanning electron micrograph of fibers after the enzymatic treatment reveals smoothened faces. The ridges that are present in the untreated fiber samples are not found in the case of cellulase-treated fibers. Bio-polishing of cotton fabrics can offer unmatched results by optimizing the process conditions, which can be otherwise achieved with chemical finishes. Reasonably good results were obtained from all the cotton and cotton blend fabrics and show high flexibility and versatility of the treatment in the manufacturing process.

This study aims to explore the incorporation of the authors previously prepared chitosan nanoparticles (CNPs) of size around 60-100 nm in the cross-linking formulation of viscose fabrics to see CNPs impact in terms of imparting multi-functional characteristics such as tensile strength, dry wrinkle recovery angles and antibacterial properties.

CNPs of size around 60-100 nm were incorporated in cross-linking formulations for viscose fabrics, including different concentrations of glutaraldehyde as a non-formaldehyde cross-linking agent and magnesium chloride hexahydrate as a catalyst. The formulations were applied at different curing times and temperatures in 100 mL distilled water, giving rise to a wet pickup of ca. 85 per cent. The fabrics were dried for 3 min at 85°C and cured at specified temperatures for fixed time intervals in thermo fixing oven according to the traditional pad-dry-cure method.

The above eco-friendly method for finished viscose fabrics was found to obtain high dry wrinkle recovery angle and maintain the tensile strength of the finished fabric within the acceptable range, as well as antibacterial properties against Escherichia coli and Staphylococcus aureus as a gram-negative and gram-positive bacteria, respectively. Both, scanning electron microscope and nitrogen percent on the finished fabric confirm the penetration of CNPs inside the fabric structure. Finally, viscose fabrics pageant antibacterial activity against gram-positive and gram-negative bacteria assessed even after 20 washing cycle.

CNPs with its flourishing effect with respect to cationic nature, biodegradability, reactivity, higher surface area and antimicrobial activity; in addition to glutaraldehyde as non-formaldehyde finishing agent can be used as multi-functional agents for viscose fabrics instead of DMDHEU, polyacrylate and monomeric composites as hazardous materials.

CNPs as cationic biopolymers were expected to impart multi-functional properties to viscose fabrics especially with obtaining reasonable dry wrinkle recovery angle and tensile strength in addition to antibacterial properties.

The novelty addressed here is undertaken with a view to impart easy care characteristics and antibacterial activities onto viscose fabrics using CNPs as antimicrobial agent and glutaraldehyde as non-formaldehyde durable press finishes to-replace the traditional formaldehyde-based resins. Besides, to the authors’ knowledge, there is no published work so far using the above cross-linking formulation written above.

Due to herbs and plants’ therapeutic properties and simplicity of availability in nature, humans have used them to treat a variety of maladies and diseases since ancient times. Later, as technology advanced, these plants and herbs gained significant relevance in some industries due to their suitable chemical composition, abundant availability and ease of access. Aegle marmelos is a species of plant that may be found in nature. Yet, little or very little literature was located on the coloration behavior of this plant’s leaves. This study aims to focus on the effect of different parameters on the extraction of colorant from Aegle marmelos leaves.

Some factors that affected on the extraction processes were examined and found to have significant impacts on the textile dyeing such as the initial dye concentration, extracted temperature, extracted bath pH and extracted time were all changed to see how they affected color extraction. The authors report a direct comparison between three heating methods, namely, microwave irradiation (MWI), ultrasonic waves (USW) and conventional heating (CH). The two kinetic models have been designed (pseudo-first and pseudo-second orders) in the context of these experiments to investigate the mechanism of the dyeing processes for fabrics under study. Also, the experimental data were analyzed according to the Langmuir and Freundlich isotherms.

From the result, it was discovered these characteristics were found to have a substantial effect on extraction efficiency. Temperature 90°C and 80°C when using CH and USW, respectively, while at 90% watt when using MWI, period 120 min when using CH as well as USW waves, while 40 min when using MWI, and pH 4, 5 and 10 for polyamide, wool and cotton, respectively, were the optimal extraction conditions. Also, the authors can say that wool gives a higher absorption than the other fabric. Additionally, MWI provided the best color strength (K/S) value, and homogeneity, at low temperatures reducing the energy and time consumed. The coloring follows the order: MWI > USW > CH. The adsorption isotherm of wool could be well fitted by Freundlich isotherm when applying CH and USW as a heating source, while it is well fitted by the Langmuir equation in the case of MWI. In the study, it was observed that the pseudo-first-order kinetic model fits better the experimental results of CH with a constant rate K₁ = −0.000171417 mg/g.min, while the pseudo-second-order kinetic model fits better the experimental results of absorption of both MWI (K2 = 38.14022572 mg/g.min) and USW (K₂ = 12.45343554 mg/g.min).

There is no research limitation for this work. Dye was extracted from Aegle marmelos leaves by applying three different heating sources (MWI, ultrasonic waves [USWW] and CH).

This work has practical applications for the textile industry. It is concluded that using Aegle marmelose leaves can be a possible alternative to extract dye from natural resource by applying new technology to save energy and time and can make the process greener.

Socially, it has a good impact on the ecosystem and global community because the extracted dye does not contain any carcinogenic materials.

The work is original and contains value-added products for the textile industry and other confederate fields.